Kamis, 17 Juli 2014









P-261
Multiplex typing of 5 Y-chromosomal SNPs

Schell D, Klein R, Miltner E, Wiegand P


Dept. of Legal Medicine, University Hospital of Ulm, Prittwitzstraße 6, 89073 Ulm


Within the last years PCR based SNP (single nucleotide polymorphism) typing has become more and more important in forensic DNA analysis. Many different methods have been established for SNP detection and especially minisequencing has often been used. In the year 2000 a new kit (SNaPshot Kit, Applied Biosystems, Darmstadt, Germany) was introduced which is based on the principle of minisequencing and especially designed for SNP detection using capillary electrophoresis. For our study we have selected 5 Y-chromosomal SNPs (M9, M17, M45, M170, M173) based on the degree of polymorphism. PCR primers were designed with the aim to get amplicon lengths   < 200 bp. The Y-SNPs were optimized in singleplex reactions and then combined to multiplex approaches by sequential optimization. Finally, we were able to analyse these 5 Y-chromosomal SNPs in one PCR/SNaPshot reaction. To validate this method for forensic stain analysis we investigated bones, bloodstains, cigarette butts and epithelial cells.  Additionally, we typed 50 unrelated Caucasian individuals to obtain our regional haplotype frequencies.


P-262
CYP2D6 polymorphism and methadone metabolism –a pharmacogenetic study

Schmid D, Anslinger K, Rolf B

Institute of Legal Medicine, Ludwigs-Maximilians-Universtiy of Munich, Munich Germany


CYP2D6 is a highly polymorphic enzyme of the cytochrome P450 family involved in the metabolism of many drugs. Due to the polymorphism of this enzyme, pharmacokinetically distinct phenotypes can be distinguished that show different enzymatic activity of the CYP2D6. For many alleles of the CYP2D6 gene, the resulting phenotype can be predicted.

Methadone is often used for substitution therapy of heroin dependence. The dose of methadone is highly variable between patients. This great interindividual variability is probably based on a pharmacokinetic difference in the phase I metabolism. It is known that the first step of methadone degradation is catalyzed by several cytochrome P450 enzymes, among others CYP2D6.

To determine the effect of CYP2D6 on the metabolism of methadone, we analysed the most common CYP2D6 polymorphism in a sample of 96 heroine abusers that were undergoing a substitution therapy with methadone.

In this sample, poor metaboliser (PM), intermediate metobolizer (IM), extensive metabolizer (EM) and ultra rapid metabolizer (UM) were observed. The phenotypes are compared to the methadone dose and the methadone concentration in the blood of the patients.

Contact: Burkhard.Rolf@med.uni-muenchen.de





P-263
Absolute DNA quantification of forensic casework samples

Schulz I, Schneider PM, Rothschild MA
Institute of Legal Medicine, University of Cologne, Germany

In forensic casework, identification systems deal with routine DNA typing of minute amounts of DNA, characteristically found in small blood stains, saliva stains, and other old or degraded biological material. Fragment size analysis using multiplex short tandem repeat (STR) systems yields excellent results from small quantities of DNA with high discrimination power. However, validation studies on the STR systems have shown that the amount of template DNA must be controlled to ensure optimal amplification and subsequent identification of the PCR product. The STR systems have an optimum DNA range of 0.5 to 2.0 ng. Thus, it is essential to determine the concentration of extracted human DNA prior to amplification. In addition to recently introduced real-time PCR methods, routine quantification of forensic samples is still predominantly done either by subjective assessment, by time- and labor-intensive slot blot procedure, or by sample-consuming and often unreliable UV-spectroscopy.
In this study, two DNA quantification methods were validated and compared in their quantification efficiency using the ABI PRISM® 7000 Sequence Detection System (SDS, Applied Biosystems). In addition to the QuantifilerTM Human DNA Quantification Kit (AB), a "home made" Telomerase Assay was designed based on sequence information provided by Applied Biosystems, and having a 98 bp target fragment. The assays are based on fluorescence resonance energy transfer and the 5’-3’ exonuclease activity of Taq DNA polymerase, respectively. Both assays detect a non-translated region of the human telomerase reverse transcriptase gene (hTERT). In contrast to the home made assay, the minor groove binder (MGB) probe of the QuantifilerTM Human DNA Quantification Kit has a length of 62 bp, and is thus 36 bp shorter than Telomerase Assay probe which is directly reflected in sensitivity differences. After establishing the within- and between-run precision, the range, the sensitivity limit and human specificity for both assays, a panel of forensic casework samples (n = 1000) was quantified, compared and investigated to assess the potential correlation with the subsequent typing results.

P-264
A novel method to quantify deleted mitochondrial DNA in a real time PCR

Schwark T, Fisch-Kohl C, von Wurmb-Schwark N

Institute of Legal Medicine, University of Kiel, Kiel, Germany


The quantification of deleted 4977 bp mitochondrial DNA (dmtDNA) may be of interest for the forensic as well as clinical pathologist. However, the determination of dmtDNA in two separate PCR reactions may lead to imprecise if not false results due to pipetting inaccuracies, deviant PCR conditions, etc. A conventional duplex PCR with subsequent fragment analysis yields only relative quantities of dmtDNA based on the analysis of PCR end products. To eliminate these factors, we established a duplex real time PCR using FAM- and VIC-labeled MGB probes. The PCR was carried out on an ABI Prism 7000 Sequence Detection System using standard chemistries. Amplicon sizes were 123 bp for deleted and 113 for total mitochondrial DNA. Serial dilutions showed a detection limit of 10 copies for both fragments.
In our opinion, the presented duplex PCR is an efficient means to reliably and easily quantify the mitochondrial 4977 bp deletion without the limitations of (conventional) singleplex PCRs.





P-265
The development of three SNP-assays for forensic casework

Senge T , Junge A , Madea B
Institute of Legal Medicine, University of Bonn, Germany

Several groups of forensic researchers work on the development of SNPs as a new marker generation for DNA classification.
The present work introduces three novel validated SNP-assays and describes their applicability in forensic casework. For this study three unlinked and non-coding SNPs named TSC0582423 (Chromosome 2), TSC0171847 (Chromosome 1) and TSC0741184 (Chromosome 3) with a balanced allele distribution were selected from the database of the SNP-consortium. SNP-detection was based on the 5'Nuclease-system from Applied Biosystems. Before the use of this SNP-detection-system in the laboratory routine, validation studies must be performed including determination of SNP-genotypes by sequencing, sensitivity studies, population studies and analysis of artificial stains. For each SNP DNA of eight unrelated persons was sequenced by Taq Cycle Sequencing to determine their SNP-alleles. These sequenced samples with known genotypes served as standard probes to establish the 5´Nuclease-assays and were used as positive controls in all analyses. For each SNP the genotype of each person determined by sequencing was identical with that determined by the 5´Nuclease-assays. Sensitivity studies were carried out with template DNA-amounts ranging from 5ng to 50pg. The test results show that an amount of at least 250pg genomic DNA could be reproducibly typed. The population studies, which were done with a group of 40 unrelated persons, show an equated allelic distribution of 58% T-Allele to 42 % C-Allele for TSC0582423, 40% T-Allele to 60% C-Allele for TSC0171847 and 59% T-Allele to 41% C-Allele for TSC0741184. The allele frequencies were comparable with those published by the SNP-consortium. The artificial stains consisted of two cigarette butts, two chewed-on chewing gums, a bottle neck abrasion as well as a scalp abrasion taken from under a fingernail. DNA extracted from the stain-material gave the expected genotypes as determined by the analysis of the corresponding saliva samples. In order to type stains with a low DNA content, an upstream multiplex PCR was developed. For each SNP a singleplex PCR with the 5´Nuclease-primers was established to get the optimal conditions for the multiplex PCR. Since only short PCR products -of about 100bp- are detected by SNP-typing using the 5´Nuclease-method, this method could be needful to detect degraded DNA. To assess the correctness of this hypothesis different approaches will be applied in the future: e.g. DNAse I-digestion and environmental studies. Also a further aspect of this work will be the comparison of the 5´Nuclease-system with the so-called Minisequencing, another method for SNP-detection, to get knowledge of the effectiveness and robustness of the two methods.

P-266
Y-STR loci multiplex amplification and haplotype analysis in a Chinese Han population

Shi MS, Li YB, Wu J, Hou YP

Department of Forensic Genetics, Sichuan University (West China University of Medical Sciences), Chengdu, P.R.China

We have developed a multiplex PCR assay dealing with simultaneously amplifying 9 STR loci on Y chromosome to aid human identity testing. These Y- STR markers included DYS434, Y-GATA-A10, DYS438, DYS439, DYS531, DYS557, DYS448, DYS456 and DYS444. Efforts were made to design three sets of the tailed primers to improve the efficiency of the multiplex PCR as well as close packing of PCR product size ranges in order to keep all alleles less than 300 bp through careful examination of known allele ranges. A total of 101 different haplotypes was found among 120 unrelated males in the Chinese Han population by using the Y-STR-9-plex system, 91 of them being unique. Gene diversity ranged from 0.4394 at DYS434 to 0.7975 at DYS557. The haplotype diversity value calculated from all nine loci combined was 0.9968. The minimum amount of input DNA that could be used to obtain a full 9 Y-STR profile was 1 ng. For the male/male mixtures, the minor component in the mixture could be identified to a ratio of 1:9. In male/female DNA mixtures, the Y-STR-9-plex proved to be highly specific for the Y chromosome in that no significant female DNA products were observed up to 300 ng of female DNA. Our results revealed that the Y-STR-9-plex system was useful for forensic analysis and paternity tests in the Chinese Han population







P-267
Characterisation of Y Chromosome SNPs Duplications

Silva MR1 , Serra S1 , Ribeiro T1 , Geada H2
1Forensic Genetics, Lisbon Delegation, National Institute of Legal Medicine
2Faculty of Medicine, University of Lisbon (hgeada@dlinml.mj.pt)

Single nucleotide polymorphisms (SNPs) have become widely used for population genetics. Multiple analysis of SNP markers can be important in future for human identity testing, specially in parentage testing and forensic casework due to low mutation rates of SNPs and analysis of 40-50 bps from heavily degraded DNA. Automation of SNP technology is also key demand.  The lack of recombination along most of the Y chromosome makes it a useful tool in male population studies and in special forensic situations, e.g., in cases of mixtures of DNA and unavailable alleged father. Furthermore, Y- SNP markers offer additional information to that obtained by STR typing. SNP typing method was based on multiplex PCR and minisequencing reaction with SNaPshotTM Multiplex Kit followed by capillary electrophoresis on an AB Prism 3100 Genetic Analyser. In a total of 102 unrelated South Portuguese males typed, 28 were from Faro District (Algarve) and 19 from Beja District. 20 Y-SNPs have been studied in three multiplex (MP) reactions – MP1/M22, P25, 92R7, SRY1532, M173, M70, Tat, M213, M9; MP2/M170, M62, M172, M26, M201; MP3/M34, M81, M78, M35, M96, M123. The most frequent haplogoup was R1b* and the haplogoup diversity was 0.6720 and 0.8304, respectively, in Faro and Beja populations. E3b1 haplogoup was only encountered in these Portuguese population samples.
In Forensic Genetics, it is important that SNP markers have only one polymorphic site for results interpretation in forensic casework. However, two of the most widely used Y-SNPs for population studies and for forensic purposes present two signals – P25 and 92R7. These duplicate segments, called Paralogous Sequence Variations (PSVs), occur in the same multiplex reaction (MP1), which at a first glance could interfere in the results interpretation. P25 polymorphism is considered to be a C-A transversion, while 92R7 is a G-A transition. These two SNP markers are implicated in the definition of the P, Q or R haplogrups in the phylogenetic tree of the Y-chromosome. Almost all samples studied presented duplication in one of these SNP markers. Two situations have been well characterised – 92R7GA, M173A, P25C for the ancient state in these SNP markers and 92R7A, M173C, P25CA for defining haplogroup R1b*(0.4901 in the Portuguese population). In very few samples characterising haplogroups R1* or R1a no duplication was detected in the two Y-SNP loci (92R7A and P25C). The polymorphism of the two Y-SNPs will be considered as C – CA for P25 and GA – A for 92R7. No P25A or 92R7G has been detected in the Portuguese population. However, in a latter African population study a 92R7G was detected, defining the ancient state as 92R7G detected in association with M173A and P25C. Another duplication was detected in the Y-SNP M78 when studying MP3. M78 polymorphism was defined as a C-T transition. While in the ancient state (M78C) the duplicated peak was in the M96 peak area, but when defining the E3b1 haplogroup (M78T), a double T peak occurred. Singleplex defined the M78 polymorphism as CC – TT.  These different types of polymorphims should be capped in mind when performing SNP typing, as by any chance, a different genetic mechanism can occur, which enable a different number of peaks in a SNP electropherogramme. Rather than an obstacle, these problems should be a challenge when using this useful new methodology for SNP typing.  
Contact: ARebelo@inml.mj.pt 

P-268
Results of the 2005 Paternity Testing Workshop of the English Speaking Working Group

Simonsen BT, Hallenberg C, Morling N

Department of Forensic Genetics, Institute of Forensic Medicine, University of Copenhagen, Denmark

Since 1991, The English Speaking Working Group (ESWG) of the International Society of Forensic Genetics (ISFG) has, once a year, offered an exercise involving genetic analysis in a paternity case. In 2005, the laboratories were invited to calculate a paper challenge in addition to performing paternity testing of a mother, two children and an alleged father. Blood samples were sent to 67 laboratories together with information about the paternity case. Also, a questionnaire concerning the techniques and routines in the laboratories were distributed.
Here, we present the results of the 2005 Paternity Testing Workshop. The evaluation includes concordance/discordance in typing results, collation of the systems used by the laboratories as well as methods used for DNA-typing. Furthermore, we present a comparison of the requirements given by the laboratories to issue a report with an excluded man and with a non-excluded man, respectively. As laboratories used different systems for typing as well as different frequency-databases in calculations, comparison of calculated PI-values in the performed paternity test was not possible. Therefore, the paper challenge constituted a valuable tool to compare calculations and to compare how laboratories deal with genetic inconsistencies, silent alleles, rare alleles as well as Y-chromosomal haplotypes. Laboratories were encouraged to treat results in the paper challenge as they would do in a paternity case as well as in an immigration case. The results of the paper challenge are presented and discussed.
[1]   Syndercombe Court D, Lincoln P, in: Carracedo A, Brinkmann B, Bär W (Eds.). A review of the 1991-1994 Paternity Testing Workshops of the English Speaking Working Group. Adv Forensic Haemogenet 1996;6:683-685.
[2]   Bjerre A, Syndercombe Court D, Lincoln P, Morling N. A report of the 1995 and 1996 Paternity Testing Workshops of the English Speaking Working Group of the International Society of Forensic Haemogenetics. Forensic Sci Int 1997; 90(1-2):41-55.
[3]   Hallenberg C, Morling N. A report of the 1997, 1998 and 1999 Paternity Testing Workshops of the English Speaking Working Group of the International Society of Forensic Genetics. Forensic Sci Int 2001;116(1):23-33.
[4]   Hallenberg C, Morling N. A report of the 2000 and 2001 Paternity Testing Workshops of the English Speaking Working Group of the International Society of Forensic Genetics. Forensic Sci Int 2002;129(1): 43-50.

P-269
Validation of multiplex STR systems for the investigation of familial relationships in immigration cases

Sippel H, Hedman M, Sajantila A

Department of Forensic Medicine, University of Helsinki, Finland
The purpose of this study was to evaluate the efficiency of three multiplex STR PCR Kits: SGM Plus and Profiler from Applied Biosystems and Penta BEC Multiplex from Promega in family reunion testing. The SGM Plus Kit is composed of the sex marker Amelogenin and 10 STR systems: D3S1358, vWA, D16S539, D2S1338, D8S1179, D21S11, D18S51, D19S433, TH01 and FGA. The second Kit, designed as Profiler combines Amelogenin and 9 STR loci: D3S1358, vWA, FGA, TH01, TPOX, CSF1PO, D5S818, D13S317, D7S820. Finally, the third kit Penta BEC Multiplex combines three STR loci, Penta B, Penta E and Penta C, and provides additional power to resolve difficult cases.
Practically any first-degree biological family relationship can be established with the same technique as that for paternity investigation. Conventional paternity testing usually assumes that the mother is the true biological mother. However, in family reunion testing the aim is to investigate whether the family is a true biological family, so there are several potential constellations, including the maternity and sibship, to test.
The paternity, maternity, sibling and avuncular indices and the likelihood ratios were calculated using the DNA-view immigration program (Brenner C, Berkeley, USA), and this calculation was based on a database constructed from the respective ethnic group. For those situations where a specific population was not available a Finnish database was used. For correcting for population substructure, an inbreeding coefficient Θ = 0.01 was used.
On the basis of this study the use of 18 STR loci is recommended for difficult familial relationship cases. Often cases with mutations, single-parent paternity cases and sibling testing without parents cannot be sufficiently resolved with SGM Plus and Profiler systems alone.

Helmuth.Sippel@helsinki.fi

P-270
Molecular variation and genetic structure of variable drug response in a worldwide population sample

Sistonen J1, Fuselli S1, Barbujani G2, Sajantila A1
1Department of Forensic Medicine, University of Helsinki, Helsinki, Finland
2Department of Biology, University of Ferrara, Ferrara, Italy

Pharmacogenetics is the study of genetically determined variation in drug response. The polymorphic Cytochrome P450 2D6 (debrisoquine 4-hydroxylase) is one of the best characterized genetic factors underlying abnormal responses to drugs. It belongs to the group of drug-metabolizing enzymes and it is responsible for about 25% of the metabolism of commonly used drugs belonging to classes like antidepressants, neuroleptics, beta-blockers and antiarrhytmics. CYP2D6 is highly polymorphic and the phenotypic consequences are considerable: the enzyme activity ranges from complete deficiency, possibly giving rise to profound toxicity of medication, to ultrarapid metabolism, which can lead to therapeutic failure with recommended drug dosages. SNPs and sequence polymorphisms of the CYP2D6 gene have been studied earlier in several populations but no systematic analysis of SNPs at the intercontinental level has been attempted to date. Here, we present the first population-genetic study of the CYP2D6 data collected in 1060 individuals from a worldwide sample of 52 populations (HGDP-CEPH panel). In the whole set of individuals, we genotyped 12 SNPs and two major rearrangements of the gene using a combination of long PCR and multiplex single base extension reaction (SNaPshot). The data was analysed to describe the geographic distribution of the gene diversity and to identify a possible spatial structure. Analyses of genetic distances and spatial autocorrelation suggest the absence of major genetic barriers and the existence of a clinal pattern. The observed partition of molecular variance shows that the percentage of global genetic variation due to intercontinental differences agrees with the value commonly obtained for neutral markers. This variation turned out to be sufficient to identify by means of a Bayesian analysis a stable population structure. Considering the relevance of CYP2D6 variation in drug metabolism and the worldwide distribution of alleles coding for enzymes with abnormal metabolic activity our results have applications in clinical as well as in forensic medicine.

P-271
Mitochondrial DNA variability in populations from East Timor (Timor Leste)

Souto L1, Rocha A M2, Pires A2, Ferreira E2, Kayser M3, Amorim A4,5, Côrte-Real F6, Vieira D N6

1Centro de Biologia Celular, Departamento de Biologia, Universidade de Aveiro, Aveiro, Portugal
2Departamento de Biologia, Universidade de Aveiro, Aveiro, Portugal
3Department of Forensic Molecular Biology, Erasmus University Medical
Centre Rotterdam, The Netherlands
4IPATIMUP, Instituto de Patologia e Imunologia Molecular da Universidade do Porto, Portugal
5Faculdade de Ciências, Universidade do Porto, Portugal
6 Delegação de Coimbra, Instituto Nacional de Medicina Legal, Coimbra, Portugal and Faculdade de Medicina da Universidade de Coimbra, Portugal.

East Timor (Timor Leste) represents a region with high linguistic diversity where two major language groups: Austronesian and non-Austronesian (or Papuan) languages are found. The purpose of our study is to reveal whether the linguistic diversity is reflected in the genetic diversity and whether genetic data can shed light into the human population history of East Timor. In this study we continue the genetic characterization of human populations from East Timor, as previously started for autosomal STRs and Y STRs, with a preliminary report on mitochondrial DNA (mtDNA) diversity. A sample of 110 individuals collected from all the districts of Timor and representing 12 linguistic groups was studied. Analyses of the mtDNA sequence from the hypervariable region 1 (HVS1) and the presence of the 9-bp deletion (intergenic regions COII-tRNA lys) were performed.
These genetic data allowed us to detect the presence of the P and Q haplogroups, typical of non-Austronesian (Papuan) speaking populations from New Guinea, along with a significant frequency of haplogroup B (namely B4a and B4b) generally associated with the expansion of Austronesian-speaking groups from East Asia along with several M sub-branches previously reported to the Southeast Asian region. Thus, our preliminary data show a correlation between linguistic and genetic diversity in East Timor and further more detailed analyses will reveal insights into the population history of the region. In addition our genetic data (mtDNA, STRs) may serve as prerequisite for forensic genetic applications in East Timor.

Contact: lsouto@bio.ua.pt 

P-272
Y-chromosome haplotypes in East Timor: evidences of population differentiation

Souto L1, Gusmão L2, Ferreira E3, Pires A3, Rocha A M3, Amorim A2,4, Côrte-Real F5,Vieira D N5

1Centro de Biologia Celular, Departamento de Biologia, Universidade de Aveiro, Aveiro, Portugal
2IPATIMUP, Instituto de Patologia e Imunologia Molecular da Universidade do Porto, Portugal
3Departamento de Biologia, Universidade de Aveiro, Aveiro, Portugal
4Faculdade de Ciências, Universidade do Porto, Portugal
5 Delegação de Coimbra, Instituto Nacional de Medicina Legal, Coimbra, Portugal and Faculdade de Medicina da Universidade de Coimbra, Portugal.

The Y-chromosome markers, due to their peculiar characteristics are considered useful tools in detecting populations’ differentiation.
The population of East Timor is known to gather a high number of ethnolinguistic groups. From linguistics and classical anthropological studies, the different groups in east Timor are generally assigned to Austronesian or Papuan ancestry.
We analysed a total of 346 males from East Timor for 12 Y-chromosome specific STRs (DYS19, DYS389I and II, DYS390, DYS391, DYS392, DYS393, DYS385, DYS437, DYS438 and DYS439). According to anthropological and linguistics information, samples were classified in major linguistic subgroups: Timoric (Timorese-Austronesian), which includes Group A (“Fabronic”, N=92) and Group A1 (“Ramelaic”, N= 130), and a third group including languages that are related to a Trans-New Guinea phylum (Papuan) and supposed to represent aboriginal (pre-austronesian) signature (Group B, N= 124).
The highest haplotype diversity value was found in Group A, “Fabronic” (0.9931), while the “Papuan” group B shows the lowest value (0.9882).
Comparison of the 3 samples suggests that the “Ramelaic” group differentiates from the “Fabronic” and “Papuan” ones (Rst values of 0.02710, P= 0.00366 and Rst of 0.05839, P= 0.0000).
These genetic results, while putting in evidence some accordance with the proposed linguistics classification, and strengthening a high homogeneity of “Papuan” speaking populations,  they also suggest that the Papuan/Austronesian linguistics criteria is not sufficient to differentiate East Timor populations and deeper analyses at ethnolinguistic groups and geographic districts should be considered.
Despite the uniqueness of the vast majority of the haplotypes found in our east Timor sample, in an extensive search in the international Y Chromosome Haplotype Reference Database (YHRD – www.yhrd.org) most of the “matches” were produced with South East Asia and Oceania samples, although “matches” with some European haplotypes were also observed.

Contacto: lsouto@bio.ua.pt 


P-273
Genotyping of human DNA recovered from mosquitoes found on a crime scene

S.Spitaleri, C. Romano, E. Ginestra  and L.Saravo*


1 Laboratory of Molecular Biology – Raggruppamento Carabinieri Investigazioni Scientifiche (RaCIS),
98128 Messina – ITALY.

Many mosquitoes species are man parasitical biters commonly found in the south of Italy by crime scene investigators. Some authors already demonstrated the possibility of amplifying human DNA from blood-meals of Diptera species using various methods for epidemiological issues. Here we decribe a casework occurred in Sicily: a person was killed in a room where no traces were found apart from a fresh mosquito blood-meal stain which could be probably referred to who had been sleeping in that place during the previous nites. Hence an optimized DNA extraction was carefully carried out in order to yield deoxyribonucleic acid uncontaminated by  insect-specific molecules. PCR amplification and STRs profiling at 15 human genetic loci was then performed on the extracted DNA, using AmpFLSTR Identifiler kit by Applied Biosystems. Additionally a DNA sample extracted from a mosquito of the same genus was processed, with equal conditions, to assess eventual unspecific detection. Results showed that it is possible to successfully amplify and obtain a complete genetic profile even if DNA is recovered from small and biologically-contamined traces. The applied analitical strategy represented a powerful tool for the investigations and allowed to address the profile to the major suspect of the murder.
Keywords: DNA STR typing; Forensic casework; Identifiler, Mosquitos.

*Corresponding author: rismebiologia@carabinieri.it

P-274

Single Human Telogen Hair Analysis: Multiplex Amplification of 8 STR loci


Spitzer E, Borck C, Grosse R

Institute of Medical Molecular Diagnostics GmbH, Schoenstrasse 90, 13086 Berlin, Germany


Hairs in the telogen phase represent the majority of trace hairs collected in connection with criminal cases. However, until now nuclear DNA profiling has not yet become routine in forensic casework because of PCR problems related to low amount and high degradation of DNA isolated from telogen hairs. There are no published procedures for efficient genotyping of single hair shafts.
Here we describe a protocol for simultaneously amplifying 8 STRs in 3 triplex amplification reactions. DNA has been purified from single hairs by phenol –chloroform extraction yielding a total of 15μl of DNA.
The primers were designed to produce amplicons of 50-150 bp. SE 33 has been excluded from triplexes due to its fragment size of 200 bp and more.
The three triplexes designated as MPX1, MPX2 and MPX3 consisted of the STRs TPOX/THO1/D18, FGA/vWA/D3, and Amelo/D8/D21 respectively. Fragment analysis has been performed by means of the 310 Genetic analyzer.
We show a number of examples to demonstrate usefulness and efficacy of the multiplex approach for single hair DNA analysis. Also, we give examples showing the necessity to perform STR typing of short DNA fragments in a special clean area apart from laboratory.
Finally, we show that our approach is suitable for other stain analysis, particularly if degraded DNA of low amounts is to be expected.

Contact: spitzer@immd.de 






P-275
Molecular analysis of genomic low copy number DNA extracted from laser-microdissected cells

N. Staiti (1), G. Giuffrè (2), D. Di Martino (1), A. Simone(2), G. Sippelli(2), G. Tuccari(2),  and L . Saravo(1)*

1 Laboratory of Molecular Biology – Raggruppamento Carabinieri Investigazioni Scientifiche (RaCIS), 98128 Messina – ITALY.
2 Department of Human Pathology, University of Messina.

Tissue microdissection techniques, allowing a correlation between the topologic organization of the cells and the molecular analysis of nucleic acids, offer the chance to characterize the several kinds of cells present both in pathologic and in forensic samples cutting small tissue fragments as well as single cells by an ultraviolet laser beam under direct microscopic visualization. The low number of target cells among a wide spectrum of cell types in heterogeneous tissue samples may complicate the analysis of biological residuals found on crime scenes, while the possibility to perform a genomic analysis of low copy number DNA from few cells harvested by laser microdissection represents a valid aid in order to solve forensic problems.
In the present report we evaluate the sensitivity of the above described method in order to perform genomic analysis from low copy number DNA. Laser-microdissection was performed using a Leica AS LMD system (Leica Microsystems, Germany) on fresh smears of aploid (spermatozoa) and diploid (lymphocytes) cells, on sections of routinely formalin-fixed and paraffin-embedded tissues, on cryostatic sections obtained at surgery and post-fixed with cold methanol. The samples were stained with specific procedures (Haematoxilin-Eosin, Giemsa, Papanicolau, Picroindigocarmine-Nuclear fast red) and an increasing number of cells (from 1 to 100) was harvested from them in different PCR tubes. DNA extraction was performed by Chelex™ 100 (Biorad), QIAmp DNA Micro Kit (Qiagen) and DNA IQ™ System (Promega Corp.). DNA extracted from each sample was amplified to identify a specific genetic profile by the most common microsatellite loci of pathologic and forensic interest. PCR products were separated by capillary electrophoresis with 3100 AB Prism Genetic Analyzer, and analyzed by Genemapper Software v 3.2 (Applera Europe B.V.).
A complete genotypic profile was obtained down to 10 aploid and 5 diploid cells as to pathological and forensic genetic markers; different results - concerning the integrity of the extracted DNA - were achieved according to the kind of histological stainings performed.                                                                                                                                  
 Keywords: DNA STR typing; Forensic casework; Mentypeâ, LMD, LCN.
*Corresponding author: rismebiologia@carabinieri.it

P-276

AZF deletions of the Y chromosome and failed amplification of commonly used Y-STRs


Stein B1, Willuweit S1, Nagy M1, Vogt PH2, Roewer L1

1Institute of Legal Medicine, Charité – University Medicine Berlin, Hannoversche Str. 6, 10115 Berlin, Germany
2Section of Molecular Genetics and Infertility, Department of Gynecological Endocrinology and Reproductive Medicine, University of Heidelberg, Im Neuenheimer Feld 328, D-69120 Heidelberg

Deletions of the Y chromosomal azoospermia factor called AZFa, AZFb and AZFc  have shown to be associated with impaired spermatogenesis. AZFc deletions are the commonest of the deletions found in infertile men, with a frequency estimated to be 1 in 4000. AZFa deletions are particularly rare (< 1 : 100 000), whereas AZFb deletions are intermediate in frequency. Sequence analysis of the complete Yq11 region reveals a 1.5 Mb overlap of the AZFb and AZFc regions (AZFb+c). Several widely used as well as new Y-STRs can be affected by the AZF deletions. For example, the multicopy Y-STR DYS464 lies within the ampliconic r1-r4 repeats of the AZFc region. The locus DYS389 resides in the AZFa region, and DYS385 and DYS392 in AZFb.
In a Y chromosomal “minimal” haplotyping study of 48 German males deleted for AZFc, AZFb and AZFb+c we found several incomplete haplotypes lacking PCR products at the loci DYS392 and DYS385. Two AZFc diagnosed male DNAs failed to amplify at the locus DYS392. This points to a wrong AZF classification, an AZFb+c deletion is more probable for this Y chromosome. One AZFb male lacks only the loci DYS385. Two AZFb males lack both DYS392 and DYS385. All three AZFb+c males show PCR failure at the loci DYS392 and DYS385. The remaining 41 AZFc diagnosed males show complete minimal haplotypes.
Recently, King et al. report deletions of DYS464 in three AZFc males (f = 3/3255) and  9 out of 19 Y-STR amplification failures for an AZFa deleted chromosome(f = 1/5374).
The core set marker set of  the Y-STR haplotype reference database (YHRD) currently includes the markers DYS19, DYS389I+II, DYS390, DYS391, DYS392, DYS393, DYS385, DYS438 and DYS439. All of these STRs are well established in forensic and genealogical routine and are included in most commercial kits. Of these STRs the markers DYS389, DYS392, DYS385, DYS438, DYS439 could fail to be amplified due to AZF deletions, thus generating incomplete haplotypes. King et al. have recommended to skip DYS464 testing for genealogical and forensic routine because of the relative high frequency of the AZFc deletion and its association with infertility. Probably because of its rarity, incomplete haplotypes pointing to the AZFa and AZFb deletions have not yet been reported to the YHRD currently comprising about 28.650 minimal and 6.281 extended haplotypes.
A consequence of inadvertent diagnosis of male infertility through genealogical or forensic Y-STR haplotyping should be information and possibly warning of customers by companies and institutions using Y-STR markers for identity testing.
Contact: lutz.roewer@charite.de

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